X-ray diffraction services: XRD.us-Price List

CATALOG NUMBER	DESCRIPTION	PRICE*
1010	Routine Sample Preparation Applies to: geological samples, minerals, soils, synthetic solid materials, pharmaceuticals etc Includes: sample handling, pulverization and mounting	$10
1020	Sample Preparation – Minimal Preferred Orientation Applies to: layered materials, fibrous, textured materials, certain polymers which are likely to be affected by preferred orientation Includes: sample handling, pulverization, sample side loading and/or spray drying	$25
1030	Sample Preparation – Enhanced Preferred Orientation Applies to: layered materials, clays, fibrous, textured materials, certain polymers which are likely to be affected by preferred orientation Includes: sample handling, pulverization, special sample loading, mounting	$25
1040	Laboratory X-ray diffractometer step-scanned data acquisition Applies to: room temperature data collection runs Includes: basic run of diffractometer	$85/hour
1050	Laboratory X-ray diffractometer step-scanned high-temperature data acquisition Applies to: data collection at elevated temperatures (up to 900^oC) Includes: air heating of sample and run of diffractometer	$95/hour
1060	Laboratory X-ray diffractometer step-scanned grazing incidence diffraction (GID) acquisition Applies to: room temperature data collection Includes: GID run of diffractometer	$110/hour
2010	Phase Identification-1 Applies to: phases with intensity of strongest peak height [I/I₁₀₀] >50%	$10/phase
2015	Phase Identification-2 Applies to: phases with intensity of strongest peak height 50% > [I/I₁₀₀] > 30%	$20/phase
2020	Phase Identification-3 Applies to: phases with intensity of strongest peak height 30% > [I/I₁₀₀] > 10%	$35/phase
2025	Phase Identification-4 Applies to: phases with intensity of strongest peak height 10% > [I/I₁₀₀]	$50/phase
3010	Quantitative Phase Analysis by Rietveld Method-1 Applies to: quantification of phases with known crystal structures and incorporated into ICSD or CCDC – unit cell, space group and coordinates of atoms or structural data supplied by customer in electronic format (e.g. CIF)	$65/phase
3015	Quantitative Phase Analysis by Rietveld Method-2 Applies to: quantification of phases with unknown crystal structures such clay minerals	$200/phase
3020	Quantitative Phase Analysis by Rietveld Method-3 Applies to: quantification of amorphous phases	$500/phase
4010	Crystallite size determination using Scherrer spherical crystal approximation	$20/phase
4020	Crystallite size distribution by Warren-Averbach Fourier series	$200/phase
4030	Precise Unit Cell Determination Applies to: novel crystalline compounds with approximately known cell parameters	$100
4040	Strain determination	$20/phase
5010	Ab initio Structure Determination with Powder Diffraction (Package) Applies to: novel crystalline compounds Includes: powder pattern indexing, space group determination, extraction of structure factor amplitudes, solutions of the structure and refinement to the acceptable R-factors. Preparation of tables for publication, a structural report, and representative drawings: ball-stick figure of unique atoms and labeling scheme, several ball-stick and polyhedral representations of structures	$300/unique atom
5015	Ab initio Structure Determination - help in preparation of publication or report Applies to: ab initio solved and refined structures Includes: Experiment, Results and Discussion on structure determination	$500/structure
6010	Rietveld Structure Refinement Applies to: any structure Includes: refinement of the structure to the acceptable R-factors. Preparation of tables for publication, a structural report, and representative drawings: ball-stick figure of unique atoms and labeling scheme, several ball-stick and polyhedral representations of structures	$80/unique atom
6015	Rietveld Structure Refinement - help in preparation of publication or report Applies to: ab initio solved and refined structures Includes: Experiment, Results and Discussion on structure determination	$500/structure
7010	Consulting Applies to: crystallography and powder diffraction Includes: phone and e-mail consultation	$100/hour
9100	Synchrotron powder diffraction data acquisition	Quoted on a project basis
9200	Neutron Powder Diffraction	Quoted on a project basis
9100	Data conversion customer-preferred formats recording on CD	$15/760MB
9200	Data conversion customer-preferred formats and transmission via e-mail or FTP	No charge
9300	XRD.US Standard Report	No charge
9400	Report, Interpretation, Presentation in customer-preferred format	Quoted on a project basis
9300	UPS and/or FedEx ground shipping of CD, printed materials and samples	As per UPS or FedEx quote

CATALOG NUMBER	DESCRIPTION	PRICE*
1110	Crystal Structure Determination Applies to: air-stable crystals Includes: Crystal mounting, data acquisition, absorption and decay corrections, cell and space group determination, data reduction, structure solution and anisotropic refinement of non-hydrogen atoms, calculated and constrained hydrogen position refinement, preparation of tables, .cif files and 1-3 drawings for publication or reporting purposes	$50/non-hydrogen atom plus $10/hydrogen atoms
1120	Laboratory single crystal X-ray diffractometer image plate data acquisition Applies to: air-stable crystals Includes: Crystal mounting, data acquisition, absorption and decay corrections, cell and space group determination, data reduction	$25/100 reflection
1130	Low Temperature surcharge Applies to: data acquisition at temperatures 290K-140K range Includes: low temperature studies	$15/non-hydrogen atom
6140	Structure Determination - help in preparation of publication or report Applies to: all solved and refined structures Includes: Experiment, Results and Discussion on structure determination	$200/structure
7110	Consulting Applies to: crystallography and single crystal diffraction Includes: phone and e-mail consultation	$100/hour
8100	Synchrotron powder diffraction data acquisition	Quoted on a project basis
8200	Neutron Powder Diffraction	Quoted on a project basis
8100	Data conversion customer-preferred formats recording on CD	$15/760MB
8200	Data conversion customer-preferred formats and transmission via e-mail or FTP	No charge
8300	XRD.US Standard Report	No charge
8400	Report, Interpretation, Presentation in customer-preferred format	Quoted on a project basis
8300	UPS and/or FedEx ground shipping of CD, printed materials and samples	As per UPS or FedEx quote